GH4169合金δ相析出与溶解行为研究

特殊钢 ›› 2021, Vol. 42 ›› Issue (5): 21-25.

所属专题：高温合金开发

GH4169合金δ相析出与溶解行为研究

白亚冠¹，李红梅¹，韩秀栋²，聂义宏³，寇金凤¹

1. 天津重型装备工程研究有限公司，天津 300457 ；
2. 天津市科学技术发展战略研究院，天津 300011 ；
3. 中国第一重型机械股份公司，齐齐哈尔 161042

收稿日期:2021-03-20 出版日期:2021-10-01 发布日期:2022-12-12
作者简介:白亚冠(1987-)，男，硕士(2011年哈尔滨工业大学)，高级工程师，2009年哈尔滨工业大学(本科)毕业，大型镍基合金及奥氏体不锈钢锻件研制。
基金资助:
天津市重点研发计划科技支撑重点项目 (18YFZCGX00220)

Study on Precipitation and Dissolution Behavior of δ Phase in GH4169 Alloy

Bai Yaguan¹,Li Hongmei¹, Han Xiudong², Nie Yihong³ , Kou Jinfeng¹

1. Tianjin Heavy Industries Research & Development Co Ltd, Tianjin 300457；
2. Tianjin Academy of Science and Technology for Development, Tianjin 300011；
3. China First Heavy Industries Machinery Co.，Ltd., Qiqihaer 161042；

Received:2021-03-20 Published:2021-10-01 Online:2022-12-12

摘要/Abstract

摘要： 研究了1050 °C 1 h固溶处理的GH4I69合金在800～980°C时效处理过程中δ相的析出行为以及900 °C 20 h预析出处理后的合金在980 ~ 1040°C固溶处理时的δ相溶解规律。研究表明,δ相的析出峰温度约为900°C ,δ相优先在晶界或率晶界析出,δ相由颗粒状长大成短棒状乃至长针状，晶内δ相由γ" 相转化而来。δ相长大方式与温度存在关系。δ相在不低于980 T的固溶处理过程中优先从δ相的交界处溶解断开，并由长针状转变为短棒状和颗粒状。晶界长针状δ相会更快的溶解，形成短棒状或颗粒状。≥ 1020 °C固溶处理可使得δ相完全溶解。

关键词: GH4169合金, δ相, 析岀, 溶解

Abstract: The precipitation behavior of δ phase of 1 050 °C 1 h solution-treated GH4169 alloy aging treated at 800 ~980 °C and the dissolution rule of δ phase in alloy after 900 °C 20 h pre-precipitation treatment alloy solution-treating at 980 ~ 1 040 °C are studied. The results indicate that the peak temperature of δ phase precipitation occurred at approximately 900 °C. δ phase precipitates in grain boundary and twin boundary first, and δ phase transforms from granular to short rod and even needle. Intragranular δ phase transforms from γ" phase. Growing up mechanism of δ phase is influenced by temperature. δ phase dissolves during no less than 980 °C solution treated from δ phase boundaries first, and then transforms from needle to short rod and granular. Needle-δ phase in grain boundary dissolves faster, and transforms to short rod or granular. The δ phase shall be completely dissolves by solution-treated at ≥1 020 °C.

白亚冠, 李红梅, 韩秀栋, 聂义宏, 寇金凤. GH4169合金δ相析出与溶解行为研究[J]. 特殊钢, 2021, 42(5): 21-25.

Bai Yaguan, Li Hongmei, Han Xiudong , Nie Yihong , Kou Jinfeng. Study on Precipitation and Dissolution Behavior of δ Phase in GH4169 Alloy[J]. Special Steel, 2021, 42(5): 21-25.

参考文献

[1] Krueger D D. The Development of Age 718 for Gas Turbine Engine Disk Applications [C]. Superalloys 718,625, 706 and Various Derivatives, Pennsylvania： The Minerals, Metals and Materials Society, 1989：279-296.
[2]Yoshida H, Hatta T and Hironaka T, et al. Process Modelling of IN718 for Free Forging [J]. AIP Conference Proceedings, 2007, 908:987-992.
[3]Ruiz C, Obabueki A and Cillespie K. Evaluation of the Microstructure and Mechanical Properties of Delta Processed Alloy 718 [C]. Superalloys 718, 625, 706 and Various Derivatives, Pennsylvania: The Minerals, Metals and Materials Society, 1992：33-42.
[4] Banik T, Mancuso S O and Maurer G E. An Evaluation of the Forgeability of Delta Processed UD1MET Alloy 718DP [C]. Superalloys 718, 625, 706 and Various Derivatives, Pennsylvania： The Minerals, Metals and Materials Society, 1994：273-280.
[5] Dix A W, Hyzak J M and Singh R P. Application of Ultra Fine Grain Alloy 718 Forging Billet [C]. Superalloys 718, 625,706 and Various Derivatives, Pennsylvania: The Minerals, Metals and Materials Society, 1992：23-32.
[6] Kuo C M, Yang Y T and Bor H Y,et al. Aging Effects on the Microstructure and Creep Behavior of Inconel 718 Superalloy [J] . Materials Science & Engineering A, 2009 , 510-511 ：289-294.
[7] Schafrik R E, Ward D D and Groh J R. Application of Alloy 718 in GE Aircraft Engines: Past, Present and Next Five Yearsf [C]. Superalloys 718, 625, 706 and Various Derivatives, Pennsylvania: The Minerals, Metals and Materials Society, 2001 ：1-11.
[8] 凌斌，钟炳文，杨玉荣，等.GH169合金的相变研究[J].航空材料学报,1994,14(4):1-7.
[9] Thomas A, Wahabi M E and Cabrera J M, et al. High Temperature Deformation of Inconel 718 [J]. Journal of Materials Processing Technology,2006,177(1-3) : 469-472.

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GH4169合金δ相析出与溶解行为研究

Study on Precipitation and Dissolution Behavior of δ Phase in GH4169 Alloy

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