Cai Qi,Jiang He,Dong Jianxin.Influence of Melting Rate and Helium Cooling on the Microstructure of GH4350 Ingots during Vacuum Arc Remelting[J].Special Steel,
Cai Qi,Jiang He,Dong Jianxin.Influence of Melting Rate and Helium Cooling on the Microstructure of GH4350 Ingots during Vacuum Arc Remelting[J].Special Steel,DOI:.
Influence of Melting Rate and Helium Cooling on the Microstructure of GH4350 Ingots during Vacuum Arc Remelting
350 mm GH4350合金铸锭真空自耗过程进行研究。主要包括不同熔炼工艺参数对熔池形状、元素宏观分布特征的影响。探究了熔速、氦冷对铸锭元素宏观分布、二次枝晶间距的影响。研究旨在采用数值模拟方法,对GH4350合金真空自耗熔炼过程进行工艺优化,对实际生产进行理论指导。研究结果表明,GH4350合金铸锭以Ti、Nb、Ta元素偏析为主。稳定期熔速对铸锭整体质量和特征具有重要影响。随着熔速提升,铸锭头部元素宏观偏析更严重,铸锭头部二次枝晶间距增大。稳定阶段熔速的变化会影响该阶段结束后的熔池体积,从而对热封顶阶段产生巨大影响,稳定阶段熔速由1 kg/min提升到5 kg/min时
350 mm GH4350 alloy ingot using MeltFlow-VAR software, integrating practical process parameters and microstructure analysis. The research focuses on the influence of various melting parameters on the molten pool profile and the macroscopic distribution of elements. Specifically, the effects of melting rate and helium cooling on the elemental macro-segregation and secondary dendrite arm spacing (SDAS) were examined . The resea
rch aims to optimize the vacuum arc remelting process of GH4350 by numerical simulation methods and provide theoretical guidance for actual production. The results indicate that the segregation of Ti, Nb, and Ta elements is predominant in the GH4350 alloy ingot. The melting rate during the stable period significantly affects the overall ingot quality and characteristics . With an increase in the melting rate, the macroscopic segregation of elements at the top of the ingot becomes more severe, and the secondary dendrite arm spacing at the ingot top also increases . Variations in the melting rate during the stable stage affect the molten pool volume at the end of this stage, thereby significantly influencing the subsequent hot topping stage. When the melting rate was raised from 1 kg/min to 5 kg/min, the maximum mass fraction of Ta element increased from 6.3% to 7.6%. With the application of 800 Pa helium cooling pressure, elemental macrosegregation was reduced, resulting in a decrease of the secondary dendrite arm spacing at the ingot center from 86 μm–115 μm to 56 μm–107 μm, and a reduction of the maximum Ta mass fraction from 7.3% to 6.5%. For elements with a high tendency to segregate, such as Ti, Nb, and Ta, the application of helium cooling significantly alleviates their macroscopic segregation
.
An increase in the melting rate has a more significant influence on the quality of the ingot compared to the absence of helium cooling.
关键词
Keywords
references
Doherty R D , Singh R P . Alloys containing gamma prime phase and particles and process for forming same : US5169463A [P]. 1992-12-08 .
SPS Technologies Aerospace Fasteners Group . Superalloys Developed by SPS Technologies for Aerospace Fasteners [R]. Jenkintown : SPS Technologies Inc , 1998
Jiang D B , Yang F Z , Zhang J , et al . Effect of feeding parameters on ingot segregation and shrinkage pore in vacuum arc remelting [J]. Journal of Iron and Steel Research International , 2023 , 30 ( 6 ): 1268 - 1278 .
Kelkar K M , Patankar S V , Mitchell A G , et al . Metals Process Simulation [M]. ASM International : FURRER D U,SEMIATIN S L , 2010 : 196 - 213 .
Kelkar K M , Patankar S V , Mitchell A G , et al . Computational modeling of the Vacuum Arc Remelting (VAR) process used for the production of ingots of Titanium alloys [C]. 11 th World Conference on Titanium , 2007 : 3 - 7
Beaman J J , Felipe Lopez L , Williamson R L . Modeling of the Vacuum Arc Remelting Process for Estimation and Control of the Liquid Pool Profile [J]. Journal of Dynamic Systems, Measurement, and Control , 2014 , 136 ( 3 ): 31007 - 31018 .
Mitchell A . Influence of process parameters during secondary melting of nickel based superalloys [J]. Materials Science and Technology , 2009 , 25 ( 2 ): 186 - 190 .
EICKHOFF M , RüCKERT A , PFEIFER H , et al . Measurement of Emission Coefficients for Alloy 718 to improve numerical simulation of industrial scale VAR Process [C]. International Conference on Modelling and Simulation of Metallurgical Processes in Steelmaking, Bardolino , 2015 , 6 .
Reiter G , Maronnier V , Sommitsch C . Numerical Simulation of the VAR Process with Calcosoft-2D and its Validation [J]. Proceedings of Liquid Metals Processing and Casting Symposium , 2003 : 77 - 86 .
Yang S L , Tian Q , Yu P , et al . Numerical simulation and experimental study of vacuum arc remelting (VAR) process for large-size GH4742 superalloy [J]. Journal of Materials Research and Technology , 2023 , 24 : 2828 - 2838 .
Nastac L . A multiscale transient modeling approach for predicting the solidification structure in VAR-processed alloy 718 ingots [J]. Metallurgical and Materials Transactions B , 2014 , 45 ( 1 ): 44 - 50 .